Information card for entry 7002968

Structure parameters

• Formula: C12 H28 I4 P2 Sn
• Calculated formula: C12 H28 I4 P2 Sn
• Title of publication: The reaction of tin(iv) iodide with phosphines: formation of new halotin anions
• Authors of publication: Apostolico, Leonardo; Kociok-Köhn, Gabriele; Molloy, Kieran C.; Blackman, Christopher S.; Carmalt, Claire J.; Parkin, Ivan P.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 47
• Pages of publication: 10486 - 10494
• a: 9.0343 ± 0.0002 Å
• b: 8.7669 ± 0.0002 Å
• c: 28.685 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2271.93 ± 0.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0498
• Residual factor for significantly intense reflections: 0.0361
• Weighted residual factors for significantly intense reflections: 0.0858
• Weighted residual factors for all reflections included in the refinement: 0.0926
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No