Crystallography Open Database

Information card for entry 7003048

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Coordinates	7003048.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C69 H50 Cl4 F6 N4 P Rh
Calculated formula	C69 H50 Cl4 F6 N4 P Rh
Title of publication	Rhodium and palladium complexes of a pyridyl-centred polyphenylene derivative
Authors of publication	Ollagnier, Cecile M. A.; Perera, Sarath D.; Fitchett, Christopher M.; Draper, Sylvia M.
Journal of publication	Dalton Transactions
Year of publication	2008
Journal issue	2
Pages of publication	283 - 290
a	24.174 ± 0.0012 Å
b	16.0642 ± 0.0008 Å
c	31.4753 ± 0.0016 Å
α	90°
β	104.943 ± 0.0011°
γ	90°
Cell volume	11809.6 ± 1 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0804
Residual factor for significantly intense reflections	0.0537
Weighted residual factors for significantly intense reflections	0.1374
Weighted residual factors for all reflections included in the refinement	0.1545
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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