Information card for entry 7003058

Structure parameters

• Formula: C102 H140 Li4 O8 P2
• Calculated formula: C102 H140 Li4 O8 P2
• Title of publication: Cubane and step-form structures of dilithium bis(aryloxy)phosphines
• Authors of publication: Carmichael, Christopher D.; Fryzuk, Michael D.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 6
• Pages of publication: 800 - 806
• a: 13.4016 ± 0.0013 Å
• b: 13.8466 ± 0.0017 Å
• c: 27.718 ± 0.003 Å
• α: 77.004 ± 0.005°
• β: 80.257 ± 0.004°
• γ: 76.333 ± 0.004°
• Cell volume: 4833.1 ± 0.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0765
• Residual factor for significantly intense reflections: 0.0533
• Weighted residual factors for significantly intense reflections: 0.1329
• Weighted residual factors for all reflections included in the refinement: 0.1462
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No