Information card for entry 7003084

Structure parameters

• Formula: C150 H169 Ga6 N12 O33.5
• Calculated formula: C150 H156 Ga6 N12 O33.5
• Title of publication: Steric control of the nuclearity of metallamacrocycles: formation of a hexanuclear gallium metalladiazamacrocycle and a hexadecanuclear manganese metalladiazamacrocycle
• Authors of publication: Lee, Kyungjin; John, Rohith P.; Park, Mira; Moon, Dohyun; Ri, Hyeong-Cheol; Kim, Ghyung Hwa; Lah, Myoung Soo
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 1
• Pages of publication: 131
• a: 16.918 ± 0.003 Å
• b: 27.325 ± 0.006 Å
• c: 16.928 ± 0.003 Å
• α: 90°
• β: 107.05 ± 0.03°
• γ: 90°
• Cell volume: 7482 ± 3 ų
• Cell temperature: 99 ± 2 K
• Ambient diffraction temperature: 99 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0905
• Residual factor for significantly intense reflections: 0.0589
• Weighted residual factors for significantly intense reflections: 0.1717
• Weighted residual factors for all reflections included in the refinement: 0.1924
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.7 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No