Information card for entry 7003162

Structure parameters

• Formula: C22 H67 Cu2 Gd K2 N4 O104 P2 W22
• Calculated formula: C22 H16 Cu2 Gd K2 N4 O82 P2 W22
• Title of publication: Organic‒inorganic hybrids assembled by bis(undecatungstophosphate) lanthanates and dinuclear copper(ii)‒oxalate complexes
• Authors of publication: Cao, Jianfang; Liu, Shuxia; Cao, Ruige; Xie, Linhua; Ren, Yuanhang; Gao, Chaoying; Xu, Lin
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 1
• Pages of publication: 115
• a: 14.747 ± 0.005 Å
• b: 20.484 ± 0.005 Å
• c: 38.466 ± 0.01 Å
• α: 90°
• β: 99.707 ± 0.007°
• γ: 90°
• Cell volume: 11453 ± 6 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 9
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0681
• Residual factor for significantly intense reflections: 0.0458
• Weighted residual factors for significantly intense reflections: 0.113
• Weighted residual factors for all reflections included in the refinement: 0.1274
• Goodness-of-fit parameter for all reflections included in the refinement: 0.951
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No