Information card for entry 7003215

Structure parameters

• Formula: C44 H40 Cl8 N2 O4 P2 Pd2
• Calculated formula: C44 H40 Cl8 N2 O4 P2 Pd2
• Title of publication: Orthopalladation of iminophosphoranes: synthesis, structure and study of stability
• Authors of publication: Bielsa, Raquel; Navarro, Rafael; Soler, Tatiana; Urriolabeitia, Esteban P.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 9
• Pages of publication: 1203 - 1214
• a: 11.9958 ± 0.0002 Å
• b: 13.5663 ± 0.0003 Å
• c: 14.8552 ± 0.0002 Å
• α: 90°
• β: 99.8661 ± 0.0014°
• γ: 90°
• Cell volume: 2381.76 ± 0.07 ų
• Cell temperature: 123 ± 1 K
• Ambient diffraction temperature: 123 ± 1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0576
• Residual factor for significantly intense reflections: 0.0456
• Weighted residual factors for significantly intense reflections: 0.0912
• Weighted residual factors for all reflections included in the refinement: 0.095
• Goodness-of-fit parameter for all reflections included in the refinement: 1.139
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No