Information card for entry 7003228

Structure parameters

• Formula: C19 H42 Cl O P2 Rh
• Calculated formula: C19 H42 Cl O P2 Rh
• Title of publication: Modelling proposed intermediates in the hydrocarbonylation of alkenes catalysed by rhodium complexes of PBui3 and PPri3
• Authors of publication: Cheliatsidou, Paraskevi; White, Daniel F. S.; Slawin, Alexandra M. Z.; Cole-Hamilton, David J.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 18
• Pages of publication: 2389 - 2394
• a: 8.0534 ± 0.0016 Å
• b: 8.875 ± 0.002 Å
• c: 16.44 ± 0.004 Å
• α: 90°
• β: 92.301 ± 0.007°
• γ: 90°
• Cell volume: 1174.1 ± 0.5 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0482
• Residual factor for significantly intense reflections: 0.0374
• Weighted residual factors for significantly intense reflections: 0.0975
• Weighted residual factors for all reflections included in the refinement: 0.1098
• Goodness-of-fit parameter for all reflections included in the refinement: 0.807
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No