Information card for entry 7003255

Structure parameters

• Formula: C61 H88 Cl4 O14 P Si7 V
• Calculated formula: C60.99 H86 Cl4 O14 P Si7 V
• Title of publication: V2O5/SiO2 surface inspired, silsesquioxane-derived oxovanadium complexes and their properties
• Authors of publication: Ohde, Christian; Brandt, Marcus; Limberg, Christian; Döbler, Jens; Ziemer, Burckhard; Sauer, Joachim
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 3
• Pages of publication: 326
• a: 10.292 ± 0.003 Å
• b: 14.543 ± 0.004 Å
• c: 24.244 ± 0.006 Å
• α: 87.33 ± 0.03°
• β: 88.66 ± 0.03°
• γ: 85.85 ± 0.03°
• Cell volume: 3614.6 ± 1.7 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2055
• Residual factor for significantly intense reflections: 0.1085
• Weighted residual factors for significantly intense reflections: 0.2673
• Weighted residual factors for all reflections included in the refinement: 0.3183
• Goodness-of-fit parameter for all reflections included in the refinement: 0.913
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No