Crystallography Open Database

Information card for entry 7003268

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Coordinates	7003268.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H46 N4 Ni
Calculated formula	C24 H46 N4 Ni
SMILES	C(C)(C)N1C(N(C(=C1C)C)C(C)C)=[Ni](=C1N(C(C)C)C(=C(C)N1C(C)C)C)(C)C
Title of publication	A method for the synthesis of nickel(0) bis(carbene) complexes
Authors of publication	Danopoulos, Andreas A.; Pugh, David
Journal of publication	Dalton Transactions
Year of publication	2008
Journal issue	1
Pages of publication	30
a	15.6502 ± 0.0002 Å
b	9.7001 ± 0.0001 Å
c	17.3931 ± 0.0002 Å
α	90°
β	104.387 ± 0.001°
γ	90°
Cell volume	2557.62 ± 0.05 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0629
Residual factor for significantly intense reflections	0.048
Weighted residual factors for significantly intense reflections	0.091
Weighted residual factors for all reflections included in the refinement	0.0986
Goodness-of-fit parameter for all reflections included in the refinement	1.08
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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