Information card for entry 7003281

Structure parameters

• Formula: C28 H54 K N4 P Si2
• Calculated formula: C28 H54 K N4 P Si2
• SMILES: [K]12[N](C)(C)CC[N]2(C)CC[N]1(C)C.[P-](C([Si](C)(C)C)[Si](C)(C)C)c4cccc5cccc(N(C)C)c45
• Title of publication: Alkali metal complexes of a naphthylamine-substituted phosphanide
• Authors of publication: Izod, Keith; Stewart, John C.; Clegg, William; Harrington, Ross W.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 3
• Pages of publication: 363
• a: 9.814 ± 0.002 Å
• b: 16.82 ± 0.004 Å
• c: 21.7 ± 0.006 Å
• α: 90°
• β: 102.932 ± 0.004°
• γ: 90°
• Cell volume: 3491.2 ± 1.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.08
• Residual factor for significantly intense reflections: 0.0449
• Weighted residual factors for significantly intense reflections: 0.0849
• Weighted residual factors for all reflections included in the refinement: 0.0999
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No