Information card for entry 7003398

Structure parameters

• Formula: C77 H94 Ga2 N4 P2 Pd
• Calculated formula: C77 H94 Ga2 N4 P2 Pd
• SMILES: [Pd]1([Ga]2N(C=CN2c2c(cccc2C(C)C)C(C)C)c2c(cccc2C(C)C)C(C)C)([P](C[P]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)[Ga]1N(C=CN1c1c(cccc1C(C)C)C(C)C)c1c(cccc1C(C)C)C(C)C
• Title of publication: Synthesis and structural characterisation of group 10 metal(ii) gallyl complexes: analogies with platinum diboration catalysts?
• Authors of publication: Jones, Cameron; Mills, David P.; Rose, Richard P.; Stasch, Andreas
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 33
• Pages of publication: 4395 - 4408
• a: 18.434 ± 0.004 Å
• b: 20.121 ± 0.004 Å
• c: 19.066 ± 0.004 Å
• α: 90°
• β: 90.89 ± 0.03°
• γ: 90°
• Cell volume: 7071 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1076
• Residual factor for significantly intense reflections: 0.0628
• Weighted residual factors for significantly intense reflections: 0.1016
• Weighted residual factors for all reflections included in the refinement: 0.1158
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No