Information card for entry 7003472

Structure parameters

• Common name: syn-((u-bpym-(4-OH))(Ru(NO)(terpy))2)(PF6)5
• Chemical name: syn-{(u-bpym-(4-OH))[Ru(NO)(terpy)]2}(PF6)5
• Formula: C76 H68 F60 N24 O11 P10 Ru4
• Calculated formula: C76 H58 F60 N24 O11 P10 Ru4
• Title of publication: Pseudo-base formation in the attempted synthesis of a conjugatively coupled bis(nitrosylruthenium) complex and spectroelectrochemistry of bipyrimidine-bridged dinuclear Ru(terpy)X precursor compounds (X = Cl, NO2)
• Authors of publication: Singh, Priti; Sieger, Monika; Fiedler, Jan; Su, Cheng-Yong; Kaim, Wolfgang
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 7
• Pages of publication: 868 - 873
• a: 10.9387 ± 0.0002 Å
• b: 26.0442 ± 0.0006 Å
• c: 19.3827 ± 0.0004 Å
• α: 90°
• β: 98.319 ± 0.001°
• γ: 90°
• Cell volume: 5463.8 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1495
• Residual factor for significantly intense reflections: 0.0979
• Weighted residual factors for significantly intense reflections: 0.1945
• Weighted residual factors for all reflections included in the refinement: 0.2181
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No