Synthetic, structural, electrochemical and solvent extraction studies of neutral trinuclear Co(ii), Ni(ii), Cu(ii) and Zn(ii) metallocycles and tetrahedral tetranuclear Fe(iii) species incorporating 1,4-aryl-linked bis-β-diketonato ligands
Authors of publication
Clegg, Jack K.; Bray, David J.; Gloe, Kerstin; Gloe, Karsten; Jolliffe, Katrina A.; Lawrance, Geoffrey A.; Lindoy, Leonard F.; Meehan, George V.; Wenzel, Marco
Journal of publication
Dalton Transactions
Year of publication
2008
Journal issue
10
Pages of publication
1331 - 1340
a
8.9493 ± 0.001 Å
b
23.585 ± 0.003 Å
c
26.145 ± 0.003 Å
α
104.688 ± 0.008°
β
93.275 ± 0.008°
γ
98.843 ± 0.007°
Cell volume
5247.9 ± 1.1 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1943
Residual factor for significantly intense reflections
0.0913
Weighted residual factors for significantly intense reflections
0.2253
Weighted residual factors for all reflections included in the refinement
0.2723
Goodness-of-fit parameter for all reflections included in the refinement
