Information card for entry 7003644

Structure parameters

• Formula: C68 H62 Cu2 N8 O9
• Calculated formula: C68 H62 Cu2 N8 O9
• Title of publication: New fluorenyl-substituted ditopic dioxotetraamine ligands and their copper(ii) complexes—synthesis, crystal structure, magnetic properties and solution behavior
• Authors of publication: Li, Qing-Xiang; Wang, Yi-Ning; Luo, Qin-Hui; Hu, Xue-Lei; Li, Yi-Zhi
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 18
• Pages of publication: 2487 - 2494
• a: 13.749 ± 0.002 Å
• b: 19.026 ± 0.003 Å
• c: 24.307 ± 0.004 Å
• α: 90°
• β: 92.51 ± 0.01°
• γ: 90°
• Cell volume: 6352.3 ± 1.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0892
• Residual factor for significantly intense reflections: 0.042
• Weighted residual factors for significantly intense reflections: 0.1109
• Weighted residual factors for all reflections included in the refinement: 0.1168
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No