Synthetic and structural investigations of alkali metal diamine bis(phenolate) complexes
Authors of publication
Clegg, William; Davidson, Matthew G.; Graham, David V.; Griffen, Gemma; Jones, Matthew D.; Kennedy, Alan R.; O'Hara, Charles T.; Russo, Luca; Thomson, Calum M.
Journal of publication
Dalton Transactions
Year of publication
2008
Journal issue
10
Pages of publication
1295 - 1301
a
15.135 ± 0.0006 Å
b
16.7141 ± 0.0006 Å
c
18.3935 ± 0.0007 Å
α
88.527 ± 0.002°
β
66.122 ± 0.002°
γ
69.106 ± 0.002°
Cell volume
3936.4 ± 0.3 Å3
Cell temperature
123 ± 2 K
Ambient diffraction temperature
123 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1311
Residual factor for significantly intense reflections
0.0617
Weighted residual factors for significantly intense reflections
0.1228
Weighted residual factors for all reflections included in the refinement
0.1521
Goodness-of-fit parameter for all reflections included in the refinement
