Information card for entry 7003679

Structure parameters

• Formula: C113 H122 B24 Cl6 N2 P6 Rh2
• Calculated formula: C113 H122 B24 Cl6 N2 P6 Rh2
• Title of publication: η1 and η2 Coordination of 1-amino-closo-dodecaborate
• Authors of publication: Kirchmann, Marius; Wesemann, Lars
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 16
• Pages of publication: 2144 - 2148
• a: 29.289 ± 0.002 Å
• b: 11.5372 ± 0.0008 Å
• c: 18.4847 ± 0.0014 Å
• α: 90°
• β: 108.395 ± 0.002°
• γ: 90°
• Cell volume: 5927.1 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1655
• Residual factor for significantly intense reflections: 0.0863
• Weighted residual factors for significantly intense reflections: 0.1522
• Weighted residual factors for all reflections included in the refinement: 0.1783
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No