Information card for entry 7003695

Structure parameters

• Formula: C36 H68 N2 Si4 Sn
• Calculated formula: C36 H68 N2 Si4 Sn
• SMILES: [Sn]12([N]([Si](C)(C)C)=C(C1[Si](C)(C)C)C13CC4CC(C1)CC(C3)C4)[N]([Si](C)(C)C)=C(C2[Si](C)(C)C)C12CC3CC(C1)CC(C2)C3
• Title of publication: Synthesis and structures of crystalline Li, Al and Sn(ii) 1-azaallyls and β-diketiminates derived from [Li{μ,η3-N(SiMe3)C(Ad)C(H)SiMe3}]2 (Ad = 1-adamantyl)
• Authors of publication: Bourget-Merle, Laurence; Hitchcock, Peter B.; Lappert, Michael F.; Merle, Philippe G.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 26
• Pages of publication: 3493 - 3501
• a: 16.1969 ± 0.0003 Å
• b: 23.3707 ± 0.0005 Å
• c: 22.0743 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8355.8 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0486
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for significantly intense reflections: 0.073
• Weighted residual factors for all reflections included in the refinement: 0.0797
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No