Crystallography Open Database

Information card for entry 7003709

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Coordinates	7003709.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C109 H109 F15 Lu N23 O19 Os S5
Calculated formula	C109 H108 F15 Lu N23 O19 Os S5
Title of publication	Towards inert and preorganized d-block-containing receptors for trivalent lanthanides: The synthesis and characterization of triple-helical monometallic OsII and bimetallic OsII‒LnIII complexes
Authors of publication	Riis-Johannessen, Thomas; Dupont, Nathalie; Canard, Gabriel; Bernardinelli, Gérald; Hauser, Andreas; Piguet, Claude
Journal of publication	Dalton Transactions
Year of publication	2008
Journal issue	28
Pages of publication	3661 - 3677
a	17.8136 ± 0.0016 Å
b	19.12 ± 0.0015 Å
c	19.1241 ± 0.0016 Å
α	75.385 ± 0.009°
β	79.682 ± 0.01°
γ	69.095 ± 0.01°
Cell volume	5859.3 ± 1 Å³
Cell temperature	150 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.049
Weighted residual factors for all reflections included in the refinement	0.048
Goodness-of-fit parameter for all reflections included in the refinement	1.54
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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