Information card for entry 7003729

Structure parameters

• Formula: C46 H42 Ag B F4 N12 O4 P2
• Calculated formula: C46 H42 Ag B F4 N12 O4 P2
• Title of publication: Supramolecular networks of silver(i) and iron(ii) complexes of the third generation tris(pyrazolyl)methane ligand Ph2(O)POCH2C(pz)3 (pz = pyrazolyl ring)
• Authors of publication: Reger, Daniel L.; Semeniuc, Radu F.; Smith, Mark D.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 17
• Pages of publication: 2253 - 2260
• a: 9.0846 ± 0.0007 Å
• b: 10.96 ± 0.0009 Å
• c: 13.914 ± 0.0012 Å
• α: 67.246 ± 0.002°
• β: 73.53 ± 0.002°
• γ: 71.977 ± 0.002°
• Cell volume: 1193.48 ± 0.17 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0663
• Residual factor for significantly intense reflections: 0.0461
• Weighted residual factors for significantly intense reflections: 0.0767
• Weighted residual factors for all reflections included in the refinement: 0.0824
• Goodness-of-fit parameter for all reflections included in the refinement: 0.937
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No