Information card for entry 7003745

Structure parameters

• Formula: C18 H23.5 B N6.5 Rh
• Calculated formula: C18 H23.5 B N6.5 Rh
• Title of publication: Solid state and solution structures of rhodium and iridium poly(pyrazolyl)borate diene complexes
• Authors of publication: Adams, Christopher J.; Anderson, Kirsty M.; Charmant, Jonathan P. H.; Connelly, Neil G.; Field, Bevis A.; Hallett, Andrew J.; Horne, Mathew
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 20
• Pages of publication: 2680 - 2692
• a: 10.8148 ± 0.0016 Å
• b: 10.1274 ± 0.0014 Å
• c: 33.316 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3649 ± 0.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 36
• Hermann-Mauguin space group symbol: C m c 21
• Hall space group symbol: C 2c -2
• Residual factor for all reflections: 0.0451
• Residual factor for significantly intense reflections: 0.0356
• Weighted residual factors for significantly intense reflections: 0.0739
• Weighted residual factors for all reflections included in the refinement: 0.0774
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No