Information card for entry 7003815

Structure parameters

• Formula: C30 H41 N Ni O P2
• Calculated formula: C30 H41 N Ni O P2
• SMILES: [Ni]12([P](C(C)C)(C(C)C)c3ccccc3N2c2ccccc2[P]1(C(C)C)C(C)C)Oc1ccccc1
• Title of publication: Terminal nickel(ii) amide, alkoxide, and thiolate complexes containing amido diphosphine ligands of the type [N(o-C6H4PR2)2]− (R = Ph, iPr, Cy)
• Authors of publication: Liang, Lan-Chang; Chien, Pin-Shu; Lee, Pei-Ying; Lin, Jia-Ming; Huang, Yu-Lun
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 25
• Pages of publication: 3320 - 3327
• a: 9.416 ± 0.0001 Å
• b: 10.777 ± 0.0002 Å
• c: 17.657 ± 0.0004 Å
• α: 98.864 ± 0.001°
• β: 93.578 ± 0.001°
• γ: 115.763 ± 0.001°
• Cell volume: 1577.45 ± 0.05 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0607
• Residual factor for significantly intense reflections: 0.0517
• Weighted residual factors for significantly intense reflections: 0.1419
• Weighted residual factors for all reflections included in the refinement: 0.1462
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No