Information card for entry 7003910

Structure parameters

• Formula: C37 H56 Cl Ge N3
• Calculated formula: C37 H56 Cl Ge N3
• SMILES: [Ge]1(Cl)[N](=C(N1c1c(cccc1C(C)C)C(C)C)N(C1CCCCC1)C1CCCCC1)c1c(cccc1C(C)C)C(C)C
• Title of publication: Synthesis, characterisation and reactivity of germanium(ii) amidinate and guanidinate complexes
• Authors of publication: Jones, Cameron; Rose, Richard P.; Stasch, Andreas
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 21
• Pages of publication: 2871 - 2878
• a: 10.586 ± 0.002 Å
• b: 18.95 ± 0.004 Å
• c: 18.311 ± 0.004 Å
• α: 90°
• β: 103.5 ± 0.03°
• γ: 90°
• Cell volume: 3571.8 ± 1.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1056
• Residual factor for significantly intense reflections: 0.0724
• Weighted residual factors for significantly intense reflections: 0.1487
• Weighted residual factors for all reflections included in the refinement: 0.1621
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No