Information card for entry 7004082

Structure parameters

• Formula: C54 H102 B30 N7 Rh3 Se6
• Calculated formula: C54 H102 B30 N7 Rh3 Se6
• Title of publication: Approaches to trinuclear half-sandwich carbene complexes containing 1,2-dicarba-closo-dodecaboranes
• Authors of publication: Xiao, Xu-Qiong; Lin, Yue-Jian; Jin, Guo-Xin
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 19
• Pages of publication: 2615 - 2619
• a: 17.031 ± 0.003 Å
• b: 17.26 ± 0.004 Å
• c: 19.256 ± 0.004 Å
• α: 110.55 ± 0.03°
• β: 98.75 ± 0.03°
• γ: 112.94 ± 0.03°
• Cell volume: 4599 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1115
• Residual factor for significantly intense reflections: 0.0563
• Weighted residual factors for significantly intense reflections: 0.1327
• Weighted residual factors for all reflections included in the refinement: 0.1473
• Goodness-of-fit parameter for all reflections included in the refinement: 0.85
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No