Information card for entry 7004101

Structure parameters

• Common name: 4 in paper
• Formula: C48 H72 O2 P2 Pd
• Calculated formula: C48 H72 O2 P2 Pd
• Title of publication: Isolation and characterization of stable, distinctly bent, trans-chelated bisphosphine palladium(0) species
• Authors of publication: Schnetz, Thomas; Röder, Marc; Rominger, Frank; Hofmann, Peter
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 17
• Pages of publication: 2238 - 2240
• a: 12.2199 ± 0.0001 Å
• b: 12.9843 ± 0.0002 Å
• c: 14.3159 ± 0.0002 Å
• α: 106.673 ± 0.001°
• β: 99.819 ± 0.001°
• γ: 90.33 ± 0.001°
• Cell volume: 2140.49 ± 0.05 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0885
• Residual factor for significantly intense reflections: 0.0471
• Weighted residual factors for significantly intense reflections: 0.091
• Weighted residual factors for all reflections included in the refinement: 0.1053
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No