Information card for entry 7004129

Structure parameters

• Formula: C29 H12 F23 O2 P
• Calculated formula: C29 H12 F23 O2 P
• Title of publication: Synthesis, structure and isomerization of arylphosphoranes with anti-apicophilic bonding modes using a novel bidentate ligand with two C2F5 groups
• Authors of publication: Jiang, Xin-Dong; Matsukawa, Shiro; Yamamoto, Yohsuke
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 28
• Pages of publication: 3678 - 3687
• a: 10.305 ± 0.0003 Å
• b: 18.221 ± 0.0006 Å
• c: 16.882 ± 0.0004 Å
• α: 90°
• β: 95.292 ± 0.003°
• γ: 90°
• Cell volume: 3156.38 ± 0.16 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1813
• Residual factor for significantly intense reflections: 0.1149
• Weighted residual factors for significantly intense reflections: 0.316
• Weighted residual factors for all reflections included in the refinement: 0.3878
• Goodness-of-fit parameter for all reflections included in the refinement: 1.109
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No