Information card for entry 7004288

Structure parameters

• Formula: C32 H56 Li4 N4
• Calculated formula: C32 H56 Li4 N4
• Title of publication: Solid-state and solution structures of hetero-aggregates formed between nBuLi and NCN pincer aryl lithium
• Authors of publication: Chase, Preston A.; Lutz, Martin; Spek, Anthony L.; Gossage, Robert A.; van Koten, Gerard
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 42
• Pages of publication: 5783 - 5790
• a: 9.4158 ± 0.0006 Å
• b: 10.4587 ± 0.0005 Å
• c: 17.6551 ± 0.0008 Å
• α: 95.909 ± 0.003°
• β: 97.918 ± 0.003°
• γ: 104.638 ± 0.003°
• Cell volume: 1648.85 ± 0.15 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0823
• Residual factor for significantly intense reflections: 0.0528
• Weighted residual factors for significantly intense reflections: 0.1257
• Weighted residual factors for all reflections included in the refinement: 0.1419
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No