Information card for entry 7004399

Structure parameters

• Formula: C39 H60 N3 Rh
• Calculated formula: C39 H60 N3 Rh
• Title of publication: Flexible coordination of bulky amidinates and guanidinates towards rhodium(i): conversion of kinetic to thermodymanic isomers
• Authors of publication: Jones, Cameron; Mills, David P.; Stasch, Andreas
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 35
• Pages of publication: 4799 - 4804
• a: 40.659 ± 0.008 Å
• b: 11.96 ± 0.002 Å
• c: 23.891 ± 0.005 Å
• α: 90°
• β: 108.9 ± 0.03°
• γ: 90°
• Cell volume: 10991 ± 4 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.068
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.1005
• Weighted residual factors for all reflections included in the refinement: 0.1129
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No