The synthesis, molecular structure and supramolecular architecture of complexes between the ammonia adduct of tris(pentafluorophenyl)boron and a series of mono and polydentate hydrogen-bond acceptors
Authors of publication
Fuller, Anna-Marie; Mountford, Andrew J.; Coles, Simon J.; Horton, Peter N.; Hughes, David L.; Hursthouse, Michael B.; Male, Louise; Lancaster, Simon J.
Journal of publication
Dalton Transactions
Year of publication
2008
Journal issue
45
Pages of publication
6381 - 6392
a
17.9464 ± 0.0003 Å
b
16.8703 ± 0.0004 Å
c
19.6562 ± 0.0003 Å
α
90°
β
106.417 ± 0.0011°
γ
90°
Cell volume
5708.51 ± 0.19 Å3
Cell temperature
120 ± 1 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0825
Residual factor for significantly intense reflections
0.0479
Weighted residual factors for significantly intense reflections
0.1017
Weighted residual factors for all reflections included in the refinement
0.1125
Goodness-of-fit parameter for all reflections included in the refinement
