Crystallography Open Database

Information card for entry 7004571

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Coordinates	7004571.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H38 N2 Pb
Calculated formula	C26 H38 N2 Pb
Title of publication	Syntheses and molecular structures of some saturated N-heterocyclic plumbylenes
Authors of publication	Charmant, Jonathan P. H.; Haddow, Mairi F.; Hahn, F. Ekkehardt; Heitmann, Dennis; Fröhlich, Roland; Mansell, Stephen M.; Russell, Christopher A.; Wass, Duncan F.
Journal of publication	Dalton Transactions
Year of publication	2008
Journal issue	43
Pages of publication	6055 - 6059
a	20.2881 ± 0.0005 Å
b	6.536 ± 0.0001 Å
c	20.2042 ± 0.0006 Å
α	90°
β	102.915 ± 0.001°
γ	90°
Cell volume	2611.36 ± 0.11 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.07
Residual factor for significantly intense reflections	0.0541
Weighted residual factors for significantly intense reflections	0.1145
Weighted residual factors for all reflections included in the refinement	0.1216
Goodness-of-fit parameter for all reflections included in the refinement	1.062
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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