Information card for entry 7004617

Structure parameters

• Formula: C76 H84 Cl14 Fe O2 P4 Zr2
• Calculated formula: C76 H84 Cl14 Fe O2 P4 Zr2
• Title of publication: Selective formation of a unique diphosphonium-diphosphine from a tetraphosphine double protonation induced by zirconium salts
• Authors of publication: Jahel, Ali; Vologdin, Nikolay V.; Pirio, Nadine; Cattey, Hélène; Richard, Philippe; Meunier, Philippe; Hierso, Jean-Cyrille
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 32
• Pages of publication: 4206 - 4208
• a: 12.302 ± 0.005 Å
• b: 18.324 ± 0.005 Å
• c: 19.112 ± 0.005 Å
• α: 75.8 ± 0.005°
• β: 89.51 ± 0.005°
• γ: 87.002 ± 0.005°
• Cell volume: 4171 ± 2 ų
• Cell temperature: 115 ± 2 K
• Ambient diffraction temperature: 115 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0899
• Residual factor for significantly intense reflections: 0.0461
• Weighted residual factors for significantly intense reflections: 0.1003
• Weighted residual factors for all reflections included in the refinement: 0.1131
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No