Information card for entry 7004702

Structure parameters

• Formula: C94 H79 F24 Fe2 N29 P4
• Calculated formula: C94 H79 F24 Fe2 N29 P4
• Title of publication: Curly‒curly, loop‒loop: homoleptic metal(ii) complexes of pyridinecarbaldehyde 4′-(2,2′:6′,2″-terpyridyl)hydrazones and their coordination polymers
• Authors of publication: Beves, Jonathon E.; Constable, Edwin C.; Housecroft, Catherine E.; Kepert, Cameron J.; Neuburger, Markus; Price, David J.; Schaffner, Silvia; Zampese, Jennifer A.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 47
• Pages of publication: 6742 - 6751
• a: 10.2902 ± 0.0002 Å
• b: 13.5226 ± 0.0003 Å
• c: 20.1859 ± 0.0004 Å
• α: 89.1662 ± 0.0009°
• β: 79.597 ± 0.0012°
• γ: 67.99 ± 0.0011°
• Cell volume: 2557 ± 0.09 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0831
• Residual factor for significantly intense reflections: 0.0459
• Weighted residual factors for all reflections: 0.0743
• Weighted residual factors for significantly intense reflections: 0.0534
• Weighted residual factors for all reflections included in the refinement: 0.0534
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1656
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No