Information card for entry 7004745

Structure parameters

• Formula: C82 H64 Cl8 Co5 N30 P S2
• Calculated formula: C82 H64 Cl8 Co5 N30 P S2
• Title of publication: First stable reduced form of [Co5]+10: fine tuning of linear pentacobalt(ii) complexes containing delocalized metal‒metal bonds through ligand modification
• Authors of publication: Wang, Wen-Zhen; Ismayilov, Rayyat Huseyn; Wang, Rui-Ren; Huang, Yi-Lin; Yeh, Chen-Yu; Lee, Gene-Hsiang; Peng, Shie-Ming
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 47
• Pages of publication: 6808 - 6816
• a: 14.806 ± 0.0004 Å
• b: 16.8778 ± 0.0004 Å
• c: 17.7166 ± 0.0005 Å
• α: 98.6556 ± 0.0015°
• β: 93.347 ± 0.0014°
• γ: 90.8523 ± 0.0016°
• Cell volume: 4368.1 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1405
• Residual factor for significantly intense reflections: 0.0728
• Weighted residual factors for significantly intense reflections: 0.1868
• Weighted residual factors for all reflections included in the refinement: 0.2226
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No