Information card for entry 7004792

Structure parameters

• Formula: C31 H54 Al2 P4 S10
• Calculated formula: C31 H54 Al2 P4 S10
• Title of publication: Aluminium complexes with thio-phosphorus ligands: syntheses and characterisations of [Al2(CyPS3)2(CyPHS2)2] and [Al(S2PPh2)3]
• Authors of publication: Davies, Robert P.; Giménez, Maria A.; Patel, Laura; White, Andrew J. P.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 42
• Pages of publication: 5705 - 5707
• a: 13.8035 ± 0.0003 Å
• b: 13.4034 ± 0.0003 Å
• c: 11.7729 ± 0.0002 Å
• α: 90°
• β: 90.7425 ± 0.0019°
• γ: 90°
• Cell volume: 2177.97 ± 0.08 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0618
• Residual factor for significantly intense reflections: 0.0433
• Weighted residual factors for significantly intense reflections: 0.0959
• Weighted residual factors for all reflections included in the refinement: 0.1071
• Goodness-of-fit parameter for all reflections included in the refinement: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No