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Information card for entry 7004889
Preview
Coordinates | 7004889.cif |
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Original paper (by DOI) | HTML |
Common name | bis((diacetyl-2-(4-N-methyl-3-thiosemicarbazonato)-3-(4'-N- methinimino-3'-thiosemicarbazonato) zinc (ii))) |
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Formula | C32 H72 N14 O8 S12 Zn2 |
Calculated formula | C32 H72 N14 O8 S12 Zn2 |
Title of publication | New bimetallic compounds based on the bis(thiosemicarbazonato) motif. |
Authors of publication | Christlieb, Martin; Cowley, Andrew R.; Dilworth, Jonathan R.; Donnelly, Paul S.; Paterson, Brett M.; Struthers, Harriet S. R.; White, Jonathan M. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2007 |
Journal issue | 3 |
Pages of publication | 327 - 331 |
a | 9.7705 ± 0.0002 Å |
b | 13.5108 ± 0.0002 Å |
c | 13.577 ± 0.0002 Å |
α | 110.932 ± 0.0008° |
β | 108.895 ± 0.0008° |
γ | 101.181 ± 0.0009° |
Cell volume | 1483.38 ± 0.05 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Sample thermal history | The material was crystallised at ambient temperature. A suitable crystal was cooled rapidly to 150K for single-crystal X-ray diffraction analysis. |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0608 |
Residual factor for significantly intense reflections | 0.0332 |
Weighted residual factors for all reflections | 0.0619 |
Weighted residual factors for significantly intense reflections | 0.0383 |
Weighted residual factors for all reflections included in the refinement | 0.0383 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.1058 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7004889.html
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