Information card for entry 7004921

Structure parameters

• Formula: C83 H101 F6 O4 P5 Pd
• Calculated formula: C83 H101 F6 O4 P5 Pd
• Title of publication: Five-coordinate Pd(II) orthometallated triarylphosphite complexes.
• Authors of publication: Bedford, Robin B.; Betham, Michael; Butts, Craig P.; Coles, Simon J.; Cutajar, Marica; Gelbrich, Thomas; Hursthouse, Michael B.; Scully, P. Noelle; Wimperis, Stephen
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 4
• Pages of publication: 459 - 466
• a: 14.3703 ± 0.0002 Å
• b: 18.2612 ± 0.0002 Å
• c: 19.3131 ± 0.0002 Å
• α: 71.258 ± 0.007°
• β: 74.58 ± 0.005°
• γ: 82.499 ± 0.005°
• Cell volume: 4621 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0987
• Residual factor for significantly intense reflections: 0.0608
• Weighted residual factors for significantly intense reflections: 0.1255
• Weighted residual factors for all reflections included in the refinement: 0.1348
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No