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Information card for entry 7004984
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Coordinates | 7004984.cif |
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Original paper (by DOI) | HTML |
Common name | [{Na(tmeda)(Me3SiNC(C6H4-Me)NPh)}2] |
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Formula | C46 H74 N8 Na2 Si2 |
Calculated formula | C46 H74 N8 Na2 Si2 |
Title of publication | Synthesis and structures of selected benzamidinates of Li, Na, Al, Zr and Sn(II) using the C1-symmetric ligands [N(SiMe3)C(C6H4Me-4 or Ph)NPh]-. |
Authors of publication | Hitchcock, Peter B.; Lappert, Michael F.; Merle, Philippe G. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2007 |
Journal issue | 5 |
Pages of publication | 585 - 594 |
a | 10.7511 ± 0.0003 Å |
b | 10.9732 ± 0.0003 Å |
c | 24.2691 ± 0.0006 Å |
α | 77.1925 ± 0.0015° |
β | 88.8729 ± 0.0016° |
γ | 63.9531 ± 0.0015° |
Cell volume | 2498.45 ± 0.12 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0658 |
Residual factor for significantly intense reflections | 0.0462 |
Weighted residual factors for significantly intense reflections | 0.1051 |
Weighted residual factors for all reflections included in the refinement | 0.1159 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.031 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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