Information card for entry 7004988

Structure parameters

• Formula: C24 H52 K N4 P Si2
• Calculated formula: C24 H52 K N4 P Si2
• Title of publication: Alkali metal complexes of sterically demanding amino-functionalized secondary phosphanide ligands.
• Authors of publication: Izod, Keith; Stewart, John C.; Clegg, William; Harrington, Ross W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 2
• Pages of publication: 257 - 264
• a: 14.4291 ± 0.0019 Å
• b: 11.2424 ± 0.0015 Å
• c: 19.756 ± 0.003 Å
• α: 90°
• β: 93.555 ± 0.002°
• γ: 90°
• Cell volume: 3198.6 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0675
• Residual factor for significantly intense reflections: 0.0531
• Weighted residual factors for significantly intense reflections: 0.1349
• Weighted residual factors for all reflections included in the refinement: 0.1486
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No