Information card for entry 7005275

Structure parameters

• Formula: C24 H30 B2 F8 Mo2 N8 O2
• Calculated formula: C24 H30 B2 F8 Mo2 N8 O2
• Title of publication: Substitution chemistry of MM quadruply bonded complexes (M = Mo or W) supported by the anion of 2-hydroxy-6-methylpyridine.
• Authors of publication: Brown, Douglas J.; Chisholm, Malcolm H.; Gribble, Christopher W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 18
• Pages of publication: 1793 - 1801
• a: 7.2615 ± 0.0001 Å
• b: 12.0539 ± 0.0002 Å
• c: 19.1113 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1672.8 ± 0.04 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 31
• Hermann-Mauguin space group symbol: P 21 n m
• Hall space group symbol: P -2 2ac
• Residual factor for all reflections: 0.0324
• Residual factor for significantly intense reflections: 0.0282
• Weighted residual factors for significantly intense reflections: 0.0671
• Weighted residual factors for all reflections included in the refinement: 0.0687
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No