Information card for entry 7005333

Structure parameters

• Formula: C33 H32 Cl2 I4 Ir2 N6 O4
• Calculated formula: C33 H32 Cl2 I4 Ir2 N6 O4
• Title of publication: Iodination of triazenide-bridged rhodium and iridium complexes: oxidative addition vs. one-electron oxidation.
• Authors of publication: Adams, Christopher J.; Baber, R. Angharad; Connelly, Neil G.; Harding, Phimphaka; Hayward, Owen D.; Kandiah, Mathivathani; Orpen, A. Guy
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 13
• Pages of publication: 1325 - 1333
• a: 8.9001 ± 0.0015 Å
• b: 9.642 ± 0.002 Å
• c: 13.51 ± 0.005 Å
• α: 94.177 ± 0.018°
• β: 100.254 ± 0.014°
• γ: 98.35 ± 0.02°
• Cell volume: 1122.9 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0448
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.0924
• Weighted residual factors for all reflections included in the refinement: 0.0969
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No