Information card for entry 7005362

Structure parameters

• Formula: C42 H53 Cl N10 Ni2 O13
• Calculated formula: C42 H53 Cl N10 Ni2 O13
• Title of publication: Ligand-controlled nuclearity in nickel bis(benzimidazolyl) complexes.
• Authors of publication: Lee, Way-Zen; Tseng, Huan-Sheng; Kuo, Ting-Shen
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 24
• Pages of publication: 2563 - 2570
• a: 16.034 ± 0.0004 Å
• b: 22.001 ± 0.0006 Å
• c: 16.185 ± 0.0005 Å
• α: 90°
• β: 104.247 ± 0.002°
• γ: 90°
• Cell volume: 5533.9 ± 0.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1578
• Residual factor for significantly intense reflections: 0.0909
• Weighted residual factors for significantly intense reflections: 0.2538
• Weighted residual factors for all reflections included in the refinement: 0.3015
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No