Information card for entry 7005524

Structure parameters

• Formula: O88.5 Rb10 Ru2 Si2 W22
• Calculated formula: O88.5 Rb10 Ru2 Si2 W22
• Title of publication: Dimerization of mono-ruthenium substituted alpha-Keggin-type tungstosilicate [alpha-SiW11O39RuIII(H2O)]5- to micro-oxo-bridged dimer in aqueous solution: synthesis, structure, and redox studies.
• Authors of publication: Sadakane, Masahiro; Tsukuma, Daisuke; Dickman, Michael H.; Bassil, Bassem S.; Kortz, Ulrich; Capron, Mickaël; Ueda, Wataru
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 26
• Pages of publication: 2833 - 2838
• a: 12.765 ± 0.0006 Å
• b: 18.9399 ± 0.001 Å
• c: 20.229 ± 0.001 Å
• α: 72.876 ± 0.003°
• β: 88.447 ± 0.003°
• γ: 80.926 ± 0.003°
• Cell volume: 4614.5 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.088
• Residual factor for significantly intense reflections: 0.0542
• Weighted residual factors for significantly intense reflections: 0.1436
• Weighted residual factors for all reflections included in the refinement: 0.1666
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No