Information card for entry 7005552

Structure parameters

• Formula: C29 H41 Br N2 Pb
• Calculated formula: C29 H41 Br N2 Pb
• SMILES: [Pb]1(Br)[N](=C(C=C(N1c1c(cccc1C(C)C)C(C)C)C)C)c1c(cccc1C(C)C)C(C)C
• Title of publication: Synthesis and theoretical studies on rare three-coordinate lead complexes.
• Authors of publication: Chen, Matthew; Fulton, J. Robin; Hitchcock, Peter B.; Johnstone, Nick C.; Lappert, Michael F.; Protchenko, Andrey V.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 26
• Pages of publication: 2770 - 2778
• a: 10.4137 ± 0.0002 Å
• b: 12.084 ± 0.0004 Å
• c: 12.4677 ± 0.0004 Å
• α: 89.224 ± 0.002°
• β: 72.815 ± 0.002°
• γ: 70.638 ± 0.002°
• Cell volume: 1407.89 ± 0.07 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0401
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.0939
• Weighted residual factors for all reflections included in the refinement: 0.0949
• Goodness-of-fit parameter for all reflections included in the refinement: 1.26
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No