Information card for entry 7005554

Structure parameters

• Formula: C38 H62 N3 Pb Si2
• Calculated formula: C38 H62 N3 Pb Si2
• Title of publication: Synthesis and theoretical studies on rare three-coordinate lead complexes.
• Authors of publication: Chen, Matthew; Fulton, J. Robin; Hitchcock, Peter B.; Johnstone, Nick C.; Lappert, Michael F.; Protchenko, Andrey V.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 26
• Pages of publication: 2770 - 2778
• a: 11.9346 ± 0.0001 Å
• b: 13.3033 ± 0.0001 Å
• c: 14.6879 ± 0.0002 Å
• α: 97.37°
• β: 100.251 ± 0.001°
• γ: 115.65 ± 0.001°
• Cell volume: 2012.46 ± 0.04 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0289
• Residual factor for significantly intense reflections: 0.025
• Weighted residual factors for significantly intense reflections: 0.0562
• Weighted residual factors for all reflections included in the refinement: 0.0578
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No