Information card for entry 7005681

Structure parameters

• Formula: C54 H53 B Br Cl2 F4 N3 O P4 W
• Calculated formula: C54 H53 B Br Cl2 F4 N3 O P4 W
• Title of publication: Extended-chain, multinuclear transition metal complexes bridged by cyanodiazenido(1-), [N=N-C[triple bond, length as m-dash]N]-, ligands.
• Authors of publication: Chan, Yun Fu; Chippindale, Ann M.; Colquhoun, Howard M.; Drew, Michael G. B.; Williams, David J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 32
• Pages of publication: 3538 - 3545
• a: 13.4062 ± 0.0003 Å
• b: 13.6587 ± 0.0003 Å
• c: 16.5249 ± 0.0005 Å
• α: 94.185 ± 0.001°
• β: 110.576 ± 0.001°
• γ: 105.646 ± 0.0013°
• Cell volume: 2680.26 ± 0.12 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 10
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1152
• Residual factor for significantly intense reflections: 0.0528
• Weighted residual factors for all reflections: 0.1075
• Weighted residual factors for significantly intense reflections: 0.0583
• Weighted residual factors for all reflections included in the refinement: 0.0584
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1188
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No