Information card for entry 7005991

Structure parameters

• Formula: C50 H70 N2 O Pb
• Calculated formula: C50 H70 N2 O Pb
• Title of publication: The synthesis of monomeric terminal lead aryloxides: dependence on reagents and conditions.
• Authors of publication: Fulton, J. Robin; Hitchcock, Peter B.; Johnstone, Nick C.; Tam, Eric C. Y.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 31
• Pages of publication: 3360 - 3362
• a: 34.4733 ± 0.0012 Å
• b: 12.0183 ± 0.0004 Å
• c: 26.7006 ± 0.0008 Å
• α: 90°
• β: 123.008 ± 0.002°
• γ: 90°
• Cell volume: 9276.8 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0509
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.0871
• Weighted residual factors for all reflections included in the refinement: 0.0927
• Goodness-of-fit parameter for all reflections included in the refinement: 1.142
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No