Crystallography Open Database

Information card for entry 7006008

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Coordinates	7006008.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C116 H148 Cl2 N56 Ni14 O42
Calculated formula	C96 H84 N56 Ni14 O22
Title of publication	The highest nuclearity metal oxime clusters: Ni14 and Ni12Na2 complexes from the use of 2-pyridinealdoximate and azide ligands.
Authors of publication	Stamatatos, Theocharis C.; Abboud, Khalil A.; Perlepes, Spyros P.; Christou, George
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	35
Pages of publication	3861 - 3863
a	17.143 ± 0.006 Å
b	20.214 ± 0.007 Å
c	25.715 ± 0.009 Å
α	83.379 ± 0.007°
β	82.208 ± 0.007°
γ	65.901 ± 0.008°
Cell volume	8041 ± 5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2199
Residual factor for significantly intense reflections	0.0828
Weighted residual factors for significantly intense reflections	0.1813
Weighted residual factors for all reflections included in the refinement	0.2042
Goodness-of-fit parameter for all reflections included in the refinement	0.603
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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