Information card for entry 7006017

Structure parameters

• Formula: C36 H100 B2 K2 N6 P2 Si4
• Calculated formula: C36 H100 B2 K2 N6 P2 Si4
• SMILES: [BH3]P(=C([Si](C)(C)C)[Si](C)(C)C)(C)C.[K]12[N](C)(C)CC[N]1(C)CC[N]2(C)C
• Title of publication: Alkali metal complexes of a phosphine-borane-stabilised carbanion: influence of co-ligands on structure.
• Authors of publication: Izod, Keith; Wills, Corinne; Clegg, William; Harrington, Ross W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 33
• Pages of publication: 3669 - 3675
• a: 21.817 ± 0.006 Å
• b: 9.323 ± 0.004 Å
• c: 29.024 ± 0.007 Å
• α: 90°
• β: 102.034 ± 0.016°
• γ: 90°
• Cell volume: 5774 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0607
• Residual factor for significantly intense reflections: 0.05
• Weighted residual factors for significantly intense reflections: 0.1348
• Weighted residual factors for all reflections included in the refinement: 0.1425
• Goodness-of-fit parameter for all reflections included in the refinement: 1.086
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No