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Information card for entry 7006039
Preview
Coordinates | 7006039.cif |
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Original paper (by DOI) | HTML |
Formula | C55.5 H43 B F15 N O4 Ti |
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Calculated formula | C55.5 H43 B F15 N O4 Ti |
Title of publication | Reactivity of boranes with a titanium(IV) amine tris(phenolate) alkoxide complex; formation of a Ti(IV) tetrahydroborate complex, a Ti(III) dimer and a Ti(IV) hydroxide Lewis acid adduct. |
Authors of publication | Johnson, Andrew L.; Davidson, Matthew G.; Mahon, Mary F. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2007 |
Journal issue | 46 |
Pages of publication | 5405 - 5411 |
a | 11.89 ± 0.0005 Å |
b | 14.543 ± 0.0004 Å |
c | 16.419 ± 0.0007 Å |
α | 108.388 ± 0.001° |
β | 100.737 ± 0.001° |
γ | 99.759 ± 0.003° |
Cell volume | 2566.42 ± 0.17 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.148 |
Residual factor for significantly intense reflections | 0.0733 |
Weighted residual factors for significantly intense reflections | 0.1727 |
Weighted residual factors for all reflections included in the refinement | 0.2095 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.024 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7006039.html
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