Information card for entry 7006212

Structure parameters

• Formula: C46 H60 Lu N O P Si2
• Calculated formula: C46 H56 Lu N O P Si2
• Title of publication: C-H activation motivated by N,N'-diisopropylcarbodiimide within a lutetium complex stabilized by an amino-phosphine ligand.
• Authors of publication: Liu, Bo; Yang, Yi; Cui, Dongmei; Tang, Tao; Chen, Xuesi; Jing, Xiabin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 38
• Pages of publication: 4252 - 4254
• a: 41.074 ± 0.003 Å
• b: 11.8955 ± 0.001 Å
• c: 19.6868 ± 0.0016 Å
• α: 90°
• β: 107.979 ± 0.001°
• γ: 90°
• Cell volume: 9149.2 ± 1.3 ų
• Cell temperature: 187 ± 2 K
• Ambient diffraction temperature: 187 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0886
• Residual factor for significantly intense reflections: 0.0523
• Weighted residual factors for significantly intense reflections: 0.0987
• Weighted residual factors for all reflections included in the refinement: 0.1106
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No