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Information card for entry 7006237
Preview
Coordinates | 7006237.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C94 H86 F6 Fe O6 P6 Pd2 S2 |
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Calculated formula | C94 H86 F6 Fe O6 P6 Pd2 S2 |
Title of publication | Dinuclear PCP pincer complexes from Lewis acidic [Pd(OTf)(PCP)] and basic [Pd(4-Spy)(PCP)] (OTf = triflate; 4-Spy = 4-pyridinethiolate; PCP = (-)CH(CH(2)CH(2)PPh(2))(2)). |
Authors of publication | Neo, Kian Eang; Huynh, Han Vinh; Koh, Lip Lin; Henderson, William; Hor, T. S. Andy |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2007 |
Journal issue | 48 |
Pages of publication | 5701 - 5709 |
a | 21.0633 ± 0.0008 Å |
b | 21.651 ± 0.0008 Å |
c | 39.0514 ± 0.0015 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 17809.1 ± 1.2 Å3 |
Cell temperature | 223 ± 2 K |
Ambient diffraction temperature | 223 ± 2 K |
Number of distinct elements | 8 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.1336 |
Residual factor for significantly intense reflections | 0.0675 |
Weighted residual factors for significantly intense reflections | 0.1507 |
Weighted residual factors for all reflections included in the refinement | 0.1768 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.993 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7006237.html
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